Cure kinetics for the acid anhydride-cured epoxy system using a near-infrared reflection spectroscopy

Geun Ho Kwak, Soo Jin Park, Jae Rock Lee

Research output: Contribution to journalArticlepeer-review

Abstract

The latent properties and cure kinetics of an acid anhydride-cured epoxy resin have been investigated by a near-infrared (NIR) reflection spectroscopy. The assignments of the latent properties and cure behaviors were performed by the measurements of the NIR reflectance for epoxide and hydroxyl groups at different temperatures. A comprehensive analysis of the origin, location, and shifts during reaction of all major NIR absorption peaks in the spectral range from 4000 to 7100 cm-1 was provided. The extent of reaction was determined from NIR absorption band at the 4530 cm-1 depending on epoxide concentration and cure temperature.

Original languageEnglish
Pages (from-to)65-71
Number of pages7
JournalPolymer (Korea)
Volume24
Issue number1
StatePublished - 2000
Externally publishedYes

Keywords

  • Cure kinetics
  • Latent properties
  • N-benzylpyrazinium hexafluaroantimonate
  • Near-infrared spectroscopy
  • Reaction mechanism

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